•  
  •  
 

Coal Geology & Exploration

Article Title

Optimization of cemented filling material ratio based on RSM-BBD method and engineering application

Abstract

In view of the problems of large stacking of solid waste caused by roof caving method in coal seam mining and imbalance between mining and filling in long-wall cemented backfilling, the No.31 ming area of Chahasu Coal Mine in Inner Monogolia uses continuous mining and filling roadway cemented backfilling mining technology, adopting the “mining at intervals of three” mining method and the “three with high strength filling and one with low strength filling” filling mode. The filling material ratio has an important influence on the filling cost and effect. In order to solve the problems of high cement consumption and less absorption of fly ash utilization in the original cemented filling materials, the optimal particle size grading coefficient n of gangue was determined based on Talbot gradation theory as 0.5, and material ratio was optimized using the Response Surface Method (RSM). Based on Box–Behnken Design (RSM-BBD) of 13 groups of tests, a regression models of the single-axis compressive strength of the backfilling body at 3, 7 and 28 days with the cement mass fraction X1, fly ash frection X2 and solid mass fraction X3, and the interaction of the three factors (X1X2, X1X3, and X2X3) was establish ed. The P values of the models were all less than 10−4, which indicates that the model has strong reliability. The test results show that not only does the single factor has a significant effect on the strength, but the interaction of factors also has a certain impact on the strength. Specifically, the strength of backfill increases with the increase of X1 and X3, but increases first and then decreases with the increase of X2. Besides, X1 has the most significant effect in the early stage, X3 has the most significant effect in the later stage, while the effect of X2 on the strength gradually becomes significant as the age period increases. X2X3 influences the 7-day strength of backfill significantly, X1X2 influences the 28-day strength significantly, and X1X3 has a significant effect on the strength at 3, 7 and 28 days. In the interaction effect of X1X3 on the strength of backfill at 7 and 28 days, the content and mass concentration of cement promote each other, capable of increasing the strength, while in the interaction, the increase of one factor will have an inhibitory effect of the other. Base on RSM, the reasonable ratio was determined as X3 at 78%‒79%, X2 at 19%‒20%; X1 at 9%‒10% for high strength filling, and X1 at 8% for low strength filling. The No.303 working face of Chahasu Coal Mine mined a total of 1.68×105 tons of coal, and consumed 1.622×105 tons of gangue , with an increase of fly ash utilization and an decrease of cement consumption of more than 1.0×104 t, greatly saving of fly ash treatment and cement cost, bringing good environmental and economic benefits.